1,15-diaza-3,4:12,13-dibenzo-5,8,11-trioxacycloheptadecane hemihydrate

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2003

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Abstract

The title compound, C20H26N2O 3·0.5H2O, contains a 17-membered diaza-crown ether ligand with three ether O and two N atoms. It consists of the macrocyclic ligand and one half water molecule; the latter possesses crystallographically imposed C2 symmetry. In the macrocyclic ring, the mean N⋯O distance is 3.995 (4) A. The macrocyclic inner hole size, estimated as twice the mean distance of the donor atoms from their centroid, is approximately 1.29 Å. © 2003 International Union of Crystallography Printed in Great Britain - all rights reserved.

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